File:Synthesis of Tetrachlorobis(diethyl ether)molybdenum(IV) - MoCl4(OEt2)2.webm

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Synthesis_of_Tetrachlorobis(diethyl_ether)molybdenum(IV)_-_MoCl4(OEt2)2.webm(WebM audio/video file, VP8/Vorbis, length 11 min 1 s, 640 × 360 pixels, 874 kbps overall)

Summary[edit]

Description

Synthesis of MoCl4(OEt2)2. In this episode, the conversion is illustrated of commercially available MoCl5 to MoCl4(OEt2)2 using tin shot as the reducing agent. The preparation is carried out by Dr. John J. Curley in the Cummins laboratory at MIT. The procedure is a modification of one reported originally by Poli et al.: Eur. J. Inorg. Chem. 2001, 2699-2703 doi:10.1002/1099-0682(200109)2001:10<2699::AID-EJIC2699>3.0.CO;2-S

Date
Source Molybdenum tetrachloride bis(diethyl ether)
Author ccclabmit

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current17:32, 20 March 201411 min 1 s, 640 × 360 (68.81 MB)Jacopo Werther (talk | contribs)== {{int:filedesc}} == {{Information |Description = Synthesis of MoCl4(OEt2)2. In this episode, the conversion is illustrated of commercially available MoCl5 to MoCl4(OEt2)2 using tin shot as the reducing agent. The preparation is carried out by Dr....
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