File:NLC416-14jh000257-62436 實用定量分析化學.pdf

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實用定量分析化學   (Wikidata search (Cirrus search) Wikidata query (SPARQL)  Create new Wikidata item based on this file)
Author
孫錫洪編
image of artwork listed in title parameter on this page
Title
實用定量分析化學
Publisher
開明書店[總發行者]
Description

目錄
第一編 定量分析入門
第一章 緒論
第一節 化學實驗
第二節 化學分析
第三節 實驗室內的常識
第四節 天秤
ⅰ 天秤的原理
ⅱ 天秤略圖說明
ⅲ 零點的測定
ⅳ 感度的測定
ⅴ 秤量
ⅵ 重量的算出
ⅶ 砝碼的補正
ⅷ 秤量上注意事項
第五節 溶液的濃度
第六節 定量分析常備試藥
ⅰ 實驗桌上自備試藥
ⅱ 實驗室內公用試藥
第七節 定量分析應備器物
第二章 重量分析
第八節 重量分析的基本操作
ⅰ 試料的採取
ⅱ 試料的溶解
ⅲ 生洇
ⅳ 濾過
ⅴ 洗滌
ⅵ 沉澱物的乾燥
ⅶ 灼熱
ⅷ 秤量
ⅸ 蒸發
ⅹ 結晶
第九節 重量分析上注意事項
ⅰ 誤差
ⅱ 分析回數
ⅲ 計算
ⅳ 清淨液
ⅴ 學習法
ⅵ 白金器具使用須知
第十節 重量分析的基本實驗
ⅰ 器物的定量
實驗1 坩鍋的恆量測定
實驗2 濾紙灰的定量
ⅱ 結晶水的定量
實驗3 硫酸銅中的結晶水定量
實驗4 氯化鋇中的結晶水定量
ⅲ 金屬的定量
實驗5 鉀盤中的鋁定量
實驗6 莫兒鹽中的鐵定量
實驗7 碳酸鈣中的鈣定量
ⅳ 酸根的定量
實驗8 鉀盤中的硫酸根定量
實驗9 食鹽中的氯定量
實驗10 磷酸氫二鈉中的磷酸根定量
第三章 容量分析
第十一節 容量分析法的分類
ⅰ 中和法
ⅱ 氧化還原法
a 高錳酸鉀法
b 重鉻酸鉀法
c 碘定量法
ⅲ 沉澱法
第十二節 容量分析的基本操作
ⅰ 測容器的使用法
ⅱ 測容器的檢定及補正
ⅲ 測容器的用途及其誤差範圍
ⅳ 標準液規定液
ⅴ 標準溶液的調製
ⅵ 指示藥
ⅶ 滴定
第十三節 容量分析上注意事項
ⅰ 誤差
ⅱ 容積的單位
ⅲ 學習法
第十四節 容量分析的基本實驗
ⅰ 中和滴定
實驗11 酸鹼定量所用標準溶液的調製
(1) 0.1n—na2co3基準溶液的調製
(2) 0.1n—hc1標準溶液的調製
(3) 0.1n—h2so4標準溶液的調製
(4) 0.1n—naoh標準溶液的調製
實驗12 酸鹼定量所用標準溶液的標定
(1) 以na2co3標定hcl
(2) 以na2co3標定h2so4
(3) 以hc1標定naoh
實驗13 食醋中的醋酸定量
實驗14 鹼灰中碳酸鈉及氫氧化鈉的定量
實驗15 硫酸銨中nh3的定量(間接法)
實驗16 水的硬度測定
ⅱ 氧化還原滴定
〔a〕 高錳酸鉀法
實驗17 高錳酸鉀法所用標準溶液的調製及標定
(1) 0.1n—h2c2o4的調製
(2) 0.1n—kmno4的調製
(3) 以naoh標定h2c2o4
(4) 以h2c2o4標定kmno4
實驗18 硫酸亞鐵銨中的鐵定量
實驗19 碳酸鈣中的鈣定量(間接法)
實驗20 二氧化二氫的定量
〔b〕 重鉻酸鉀法
實驗21 重鉻酸鉀法所用標準溶液的調製及標定
(1) 0.1n—k2cr2o7的調製
(2) 以na2s2o3標定k2cr2o7
實驗22 鐵銨盤中的鐵定量
實驗23 鉻鐵礦中的鉻定量
〔c〕 碘定量法
實驗24 碘定量法所用標準溶液的調製及標定
(1) 0.1n—na2s2o3的調製
(2) 0.1n—i3的調製
(3) 以kmno4標定na2s2o3
(4) 以na2s2o3標定i2
實驗25 硫酸銅中的銅定量
實驗26 亞砷酸中的砷定量
實驗27 漂白粉中的有效氯定量
ⅲ 沉澱滴定
實驗28 沉澱法所用標準溶液的調製及標定
(1) 0.1n—agno3的調製
(2) 0.1n—nacl
(3) 以純銀標定nacl
(4) 以nacl標定agno3
實驗29 用水中的氯定量
實驗30 氰化鉀的定量
第二編 定量分析應用
第四章 工業分析
第十五節 合金分析
實驗31 銅合金的分析
實驗32 鋼鐵的分析
第十六節 礦物分析
實驗33 碳酸礦的分析
實驗34 硫黃礦的分析
實驗35 不溶硅酸鹽的分析
第十七節 水的分析
實驗36 飲料用水的分析
第十八節 電解分析
實驗37 真鑰的分析
第十九節 燃料分析
實驗38 煤的分析
第二十節 氣體分析
實驗39 煤氣的分析
實驗40 煙道氣體的分析
實驗41 亞硝酸及硝酸的定量
第二十一節 元素分析
實驗42 碳氫氧的測定
第二十二節 有機物及其製造品分析
實驗43 油脂的分析
實驗44 肥皂的分析
實驗45 膠皮的分析
實驗46 牛乳的分析
實驗47 糖的分析
實驗48 酒的分析
附錄
ⅰ 本書常各略號一覽
ⅱ 沉澱物灼熱的溫度
ⅲ 化學用玻璃的分析表
ⅳ 無機化學分析參考書
原子周期表
萬國原子量表
溶解度表

Language Chinese
Publication date 民國三十二年[1943]
Source
institution QS:P195,Q732353
(民國時期文獻 民國圖書)
館藏信息
InfoField
MG/0655/3
主題
InfoField
定量分析
中圖分類
InfoField
O655
載體形態
InfoField
196頁

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current09:44, 11 June 2023Thumbnail for version as of 09:44, 11 June 2023835 × 1,204, 214 pages (7.38 MB)PencakeBot (talk | contribs)Upload 實用定量分析化學 (1/1) by 孫錫洪編 (batch task; nlc:data_416,14jh000257,62436; 民國圖書.8; 實用定量分析化學)

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